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A hydrophobic silica fine powder is prepared by premixing a hydrophilic silica fine powder with a dimer diol siloxane or cyclic siloxane as a hydrophobizing agent, mixing them in a ball mill for achieving dispersion and for achieving cleavage or disintegration and consolidation, and thereafter heating at 100-300° C. in an ammonia or amine-containing atmosphere.
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Ball mills, like the three roll machine, are a common occurrence in industry, for the production of fine particles. During the ball milling process, there are two factors that contribute to the exfoliation. The main factor contributing is the shear force applied by the balls. Using only shear force, one can produce large graphene flakes.
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A method and apparatus for making highly pure silica powder by milling the substantially pure SiO 2 charge in a ball mill which is made with an interior lining of contiguous silicon nitride plates or tiles and which employs silicon nitride media. The silicon nitride plates and media prevent contamination of the silica charge while minimizing their deterioration.
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